| Designation Number | Year Discontinued | Title | Replaced By: |
| D2554 | 1992 | Method of Test for Flash Point of Drycleaning Detergents in the Drycleaning Bath | |
| D2762 | 1992 | Specification for Drycleaning Detergent, Non-Charge Type | |
| D2763 | 1992 | Specification for Drycleaning Detergent, Liquid Charge Type | |
| D4224 | 1995 | Test Method for Anionic Detergent By Para-Toluidine Hydrochloride | D4251 |
| D2553 | 1992 | Method of Test for Detecting Odor of Drycleaning Detergent on a Drycleaned Garment | |
| D2760 | 2000 | Test Method for Analysis of Sodium Triphosphate by the Simplified Paper Chromatographic Method | |
| D1279 | 1999 | Test Method for Buffering Action of Metal Cleaners | |
| D1374 | 2000 | Test Method of Aerated Total Immersion Corrosion Test for Metal Cleaners | |
| D1567 | 2000 | Test Method for Detergent Cleaners for Evaluation of Corrosive Effects on Certian Porcelain Enamels | |
| D455 | 2000 | Specification for Milled Toilet Soap | |
| D496 | 2000 | Specification for Chip Soap | |
| D497 | 2000 | Specification for Ordinary Laundry Bar Soap | |
| D498 | 2000 | Specification for Powdered Soap (Nonalkaline Soap Powder) | |
| D499 | 2000 | Specification for White Floating Toilet Soap | |
| D533 | 2000 | Specification for Built Soap, Powdered | |
| D534 | 2000 | Specification for Alkaline Soap Powder | |
| D799 | 2000 | Specification for Liquid Toilet Soap | |
| D2021 | 2000 | Specification for Neutral Detergent, 40 Percent Alkylbenzene Sulfonate Type | |
| D2179 | 2000 | Specification for Combination Bar Soap | |
| D2356 | 2000 | Specification for Phosphate and Silica Containing Scouring Powder Compounds | |
| D2955 | 2000 | Specification for Hand Scrubbing Soap (Grit Soap) Powder | |
| D2957 | 2000 | Specification for Hand Scrubbing Soap (Grit Soap) Powder | |
| D2958 | 2000 | Specification for Powdered Toilet Soap | |
| D3047 | 2000 | Specification for Powdered Hand Cleaner (Soap With Vegetable Scrubber) | |
| D3399 | 2000 | Specification for General-Purpose Synthetic Detergent Liquid | |
| D3494 | 2000 | Specification for Water-Emulsion Floor Polish Remover | |
| D4010 | 2000 | Specification for Waterless Hand Cleaner | |
| D4011 | 2000 | Specification for Lotion Soap | |